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Proposition of methods for direct analysis of electronic waste samples: determination of precious, strategic and toxic elements in printed circuits boards and LCD screens

Grant number: 16/17304-0
Support type:Scholarships in Brazil - Doctorate
Effective date (Start): April 01, 2017
Effective date (End): March 31, 2021
Field of knowledge:Physical Sciences and Mathematics - Chemistry - Analytical Chemistry
Principal researcher:Edenir Rodrigues Pereira Filho
Grantee:Daniel Fernandes de Andrade
Home Institution: Centro de Ciências Exatas e de Tecnologia (CCET). Universidade Federal de São Carlos (UFSCAR). São Carlos , SP, Brazil
Associated scholarship(s):18/24569-6 - Direct element characterization of mobile phones using data fusion from three complementary spectroanalytical techniques, BE.EP.DR

Abstract

Advances in technological development have resulted in a high consumption of electrical and electronic equipment, including cell phones and computers that are composed primarily by printed circuit boards (PCBs), liquid cristal display (LCD) screens, batteries and other components. With the frequent renewal of these products, e-waste is among the fastest growing waste in the world. In this context, the proposed research project seeks the development of analytical procedures for direct analysis of electronic waste samples of difficult preparation using laser-induced breakdown spectroscopy (LIBS) and wavelength dispesive X-ray fluorescence (WD-XRF). This proposal is relevant in several aspects, since it covers studies related to the preparation of important samples to be monitored, as well as the application of spectrochemical and chemometric tools to solve analytical problems of national interest. Several methodologies will be applied for determination of precious (Au and Ag), toxic (Cd, Cr and Pb) and strategic (Pd, Pt, In and Ta) elements in PCBs and LCD screens, from mobile phones and computers discarded with no reuse intention. The development of these studies can contribute to applications of LIBS and WD-XRF to complex matrices, enabling research strategies to eliminate possible interference, and thus establish a methodology with similar analytical performance or better than the existing alternatives.

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Scientific publications (24)
(References retrieved automatically from Web of Science and SciELO through information on FAPESP grants and their corresponding numbers as mentioned in the publications by the authors)
COSTA, VINICIUS CAMARA; CASTRO, JEYNE PRICYLLA; ANDRADE, DANIEL FERNANDES; BABOS, DIEGO VICTOR; GARCIA, JOSE AUGUSTO; SPERANCA, MARCO AURELIO; CATELANI, TIAGO AUGUSTO; PEREIRA-FILHO, EDENIR RODRIGUES. Laser-induced breakdown spectroscopy (LIBS) applications in the chemical analysis of waste electrical and electronic equipment (WEEE). TRAC-TRENDS IN ANALYTICAL CHEMISTRY, v. 108, p. 65-73, . (16/17221-8, 16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; SPERANCA, MARCO AURELIO; PEREIRA-FILHO, EDENIR RODRIGUES. Different sample preparation methods for the analysis of suspension fertilizers combining LIBS and liquid-to-solid matrix conversion: determination of essential and toxic elements. ANALYTICAL METHODS, v. 9, n. 35, p. 5156-5164, . (15/14488-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; ROMANELLI, JOAO PAULO; PEREIRA-FILHO, EDENIR RODRIGUES. Past and emerging topics related to electronic waste management: top countries, trends, and perspectives. Environmental Science and Pollution Research, v. 26, n. 17, p. 17135-17151, . (16/01513-0, 16/17304-0)
MACHADO, RAQUEL C.; SILVA, ANA BEATRIZ S.; ANDRADE, DANIEL F.; PINHEIRO, FERNANDA C.; WILLIAMS, CHARLES B.; DONATI, GEORGE L.; NOGUEIRA, ANA RITA A.; PEREIRA-FILHO, EDENIR R.. Alternative Approaches Applied to Inductively Coupled Plasma Techniques: Multi-Flow and Two-Flow Calibration. Journal of the Brazilian Chemical Society, v. 32, n. 4, p. 842-851, . (18/26145-9, 19/24223-5, 16/17304-0)
ANDRADE, DANIEL FERNANDES; GUEDES, WESLEY NASCIMENTO; VERBI PEREIRA, FABIOLA MANHAS. Detection of chemical elements related to impurities leached from raw sugarcane: Use of laser-induced breakdown spectroscopy (LIBS) and chemometrics. Microchemical Journal, v. 137, p. 443-448, . (16/00779-6, 16/17304-0)
MACHADO, RAQUEL C.; ANDRADE, DANIEL F.; BABOS, V, DIEGO; CASTRO, JEYNE P.; COSTA, VINICIUS C.; SPERANCA, MARCO AURELIO; GARCIA, JOSE AUGUSTO; GAMELA, RAIMUNDO R.; PEREIRA-FILHO, EDENIR R.. Solid sampling: advantages and challenges for chemical element determination-a critical review. Journal of Analytical Atomic Spectrometry, v. 35, n. 1, p. 54-77, . (16/17221-8, 16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; MACHADO, RAQUEL CARDOSO; BACCHI, MARCIO ARRUDA; PEREIRA-FILHO, EDENIR RODRIGUES. Proposition of electronic waste as a reference material - part 1: sample preparation, characterization and chemometric evaluation. Journal of Analytical Atomic Spectrometry, v. 34, n. 12, p. 2394-2401, . (16/01513-0, 16/17304-0)
VINICIUS C. COSTA; AMANDA S. AUGUSTO; JEYNE P. CASTRO; RAQUEL C. MACHADO; DANIEL F. ANDRADE; DIEGO V. BABOS; MARCO A. SPERANÇA; RAIMUNDO R. GAMELA; EDENIR R. PEREIRA-FILHO. LASER INDUCED-BREAKDOWN SPECTROSCOPY (LIBS): HISTÓRICO, FUNDAMENTOS, APLICAÇÕES E POTENCIALIDADES. Química Nova, v. 42, n. 5, p. 527-545, . (16/17304-0, 16/17221-8, 14/11415-0, 16/01513-0)
ROMANELLI, JOAO PAULO; GONCALVES, MARIA CAROLINA PEREIRA; DE ABREU PESTANA, LUIS FERNANDO; SOARES, JESSICA AKEMI HITAKA; BOSCHI, RAQUEL STUCCHI; ANDRADE, DANIEL FERNANDES. Four challenges when conducting bibliometric reviews and how to deal with them. Environmental Science and Pollution Research, v. 28, n. 43, . (13/50718-5, 19/23908-4, 19/08533-4, 18/18416-2, 16/17304-0)
SANTANA, ANA P. R.; ANDRADE, DANIEL F.; GUIMARAES, TACIANA G. S.; AMARAL, CLARICE D. B.; OLIVEIRA, ANDREA; GONZALEZ, MARIO H.. Synthesis of natural deep eutectic solvents using a mixture design for extraction of animal and plant samples prior to ICP-MS analysis. Talanta, v. 216, . (15/08873-9, 17/18531-3, 16/17304-0)
CASTRO, JEYNE PRICYLLA; SPERANCA, MARCO AURELIO; BABOS, DIEGO VICTOR; ANDRADE, DANIEL FERNANDES; PEREIRA-FILHO, EDENIR RODRIGUES. Neodymium determination in hard drive disks magnets using different calibration approaches for wavelength dispersive X-ray fluorescence. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v. 164, . (16/01513-0, 16/17304-0, 16/17221-8, 18/17753-5, 14/22408-4, 12/01769-3)
ANDRADE, DANIEL FERNANDES; CASTRO, JEYNE PRICYLLA; GARCIA, JOSE AUGUSTO; MACHADO, RAQUEL CARDOSO; PEREIRA-FILHO, EDENIR RODRIGUES; AMARASIRIWARDENA, DULASIRI. Analytical and reclamation technologies for identification and recycling of precious materials from waste computer and mobile phones. Chemosphere, v. 286, n. 2, . (16/17304-0, 16/17221-8, 18/24569-6, 19/24223-5)
BABOS, DIEGO VICTOR; CASTRO, JEYNE PRICYLLA; ANDRADE, DANIEL FERNANDES; COSTA, VINICIUS CAMARA; PEREIRA-FILHO, EDENIR RODRIGUES. Determination and speciation of phosphorus in fertilizers and mineral supplements for cattle by X-ray absorption near-edge structure spectroscopy: a simple nondestructive method. ANALYTICAL METHODS, v. 11, n. 11, p. 1508-1515, . (16/17221-8, 16/01513-0, 16/17304-0)
GAMELA, RAIMUNDO R.; SPERANCA, MARCO A.; ANDRADE, DANIEL F.; PEREIRA FILHO, EDENIR R.. Hyperspectral images: a qualitative approach to evaluate the chemical profile distribution of Ca, K, Mg, Na and P in edible seeds employing laser-induced breakdown spectroscopy. ANALYTICAL METHODS, v. 11, n. 43, p. 5543-5552, . (16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; FORTUNATO, FELIPE MANFROI; PEREIRA-FILHO, EDENIR RODRIGUES. Calibration strategies for determination of the In content in discarded liquid crystal displays (LCD) from mobile phones using laser-induced breakdown spectroscopy (LIBS). Analytica Chimica Acta, v. 1061, p. 42-49, . (16/01513-0, 16/17304-0)
ANDRADE, DANIEL FERNANDES; PEREIRA-FILHO, EDENIR RODRIGUES; AMARASIRIWARDENA, DULASIRI. Current trends in laser-induced breakdown spectroscopy: a tutorial review. APPLIED SPECTROSCOPY REVIEWS, v. 56, n. 2, . (18/24569-6, 16/01513-0, 16/17304-0)
SPERANCA, MARCO AURELIO; ANDRADE, DANIEL FERNANDES; CASTRO, JEYNE PRICYLLA; PEREIRA-FILHO, EDENIR RODRIGUES. Univariate and multivariate calibration strategies in combination with laser-induced breakdown spectroscopy (LIBS) to determine Ti on sunscreen: A different sample preparation procedure. OPTICS AND LASER TECHNOLOGY, v. 109, p. 648-653, . (16/01513-0, 16/17304-0, 16/17221-8)
ALEXANDRINA, EDUARDO CARLOS; BABOS, DIEGO VICTOR; ANDRADE, DANIEL FERNANDES; COSTA, VINICIUS CAMARA; LUI, ELAINE SCHORNOBAY; CORREA, NIVALDO APARECIDO; AGUIAR, MONICA LOPES; PEREIRA-FILHO, EDENIR RODRIGUES. Particulate matter (PM10) from Sao Carlos-SP (Brazil): spectroanalytical techniques to evaluate and determine chemical elements. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, v. 99, n. 7, . (16/01513-0, 12/14928-2, 16/17304-0)
ANDRADE, DANIEL FERNANDES; DE ALMEIDA, EDUARDO; PEREIRA DE CARVALHO, HUDSON WALLACE; PEREIRA-FILHO, EDENIR RODRIGUES; AMARASIRIWARDENA, DULASIRI. Chemical inspection and elemental analysis of electronic waste using data fusion - Application of complementary spectroanalytical techniques. Talanta, v. 225, . (16/01513-0, 15/05942-0, 16/17304-0, 18/24569-6, 19/24223-5)
VINICIUS C. COSTA; DIEGO V. BABOS; JEYNE P. CASTRO; DANIEL F. ANDRADE; RAIMUNDO R. GAMELA; RAQUEL C. MACHADO; MARCO A. SPERANÇA; ALISSON S. ARAÚJO; JOSÉ A. GARCIA; EDENIR R. PEREIRA-FILHO. Calibration Strategies Applied to Laser-Induced Breakdown Spectroscopy: A Critical Review of Advances and Challenges. Journal of the Brazilian Chemical Society, v. 31, n. 12, p. 2439-2451, . (18/24569-6, 16/01513-0, 16/17221-8, 19/24223-5, 18/17753-5, 16/17304-0)
MACHADO, RAQUEL C.; BABOS, DIEGO VICTOR; ANDRADE, DANIEL F.; PEREIRA-FILHO, EDENIR RODRIGUES. A novel strategy for direct elemental determination using laser-induced breakdown spectroscopy: fluence calibration. Journal of Analytical Atomic Spectrometry, v. 36, n. 10, . (16/17304-0, 19/24223-5, 16/01513-0)
ANA P. R. SANTANA; DANIEL F. ANDRADE; TACIANA G. S. GUIMARÃES; CLARICE D. B. AMARAL; ANDREA OLIVEIRA; ANA R. A. NOGUEIRA; MARIO H. GONZALEZ. Solventes eutéticos naturais profundos (NADES) no preparo de amostras de rocha fosfática e suplemento mineral para determinação elementar por técnicas de plasma. Química Nova, v. 44, n. 6, p. 689-695, . (16/17304-0, 15/14488-0, 19/22113-8, 17/18531-3)
ANDRADE, DANIEL FERNANDES; MACHADO, RAQUEL CARDOSO; PEREIRA-FILHO, EDENIR RODRIGUES. Proposition of electronic waste as a reference material - part 2: homogeneity, stability, characterization, and uncertainties. Journal of Analytical Atomic Spectrometry, v. 34, n. 12, p. 2402-2410, . (16/01513-0, 16/17304-0)
GUIMARAES, TACIANA G. S.; ANDRADE, DANIEL F.; SANTANA, ANA P. R.; MOSER, POLIANA; FERREIRA, SABRINA S.; MENEZES, IOHANNA M. N. R.; AMARAL, CLARICE D. B.; OLIVEIRA, ANDREA; GONZALEZ, MARIO H.. Mixture design and physicochemical characterization of amino acid-based DEEP eutectic solvents (AADES) for sample preparation prior to elemental analysis. JOURNAL OF MOLECULAR LIQUIDS, v. 345, . (14/50945-4, 15/14488-0, 12/23066-4, 16/17304-0, 19/22113-8)

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